气相色谱-质谱法测定白酒中挥发性成分Analysis of Volatile Components in Distillate Spirit by Gas Chromatography-Mass Spectrometry
胡朝阳,裘璐,肖海涛
HU Chaoyang,QIU Lu,XIAO Haitao(School of Pharmacology
摘要(Abstract):
目的:研究酒中的挥发性成分。方法:采用气相色谱-质谱(GC-MS)联用技术对酒中的挥发性成分进行分析鉴定,用色谱峰面积归一化法计算各成分的相对含量。结果:从所检酒中鉴定出11个挥发性成分,占总挥发性成分相对含量的97.98%,其中主要成分为酯类(49.48%)、醛类(19.27%)、有机酸(18.17%)和醇类(8.92%)。结论:本研究为某白酒的香型和风格定性提供了依据。
Objective: To study the volatile components in distillate spirit.Methods: A combined method of gas chromatography and mass spectrometry(GC-MS) was used to analyze and identify the volatile components in distillate spirit.The relative contents of individual components were determined with area normalization method.Results: Eleven constituents in distillate spirit were identified,which occupied 97.98% of total volatile components.The main constituents were esters(49.48 %),aldehydes(19.27 %),organic acid(18.17 %),and spirits(8.92 %).Conclusion: This research provides a qualitative evidence for flavor and style of distillate spirit.
关键词(KeyWords):
色谱法,气相;脂肪酸类,挥发性;红星二锅头;挥发性成分
chromatography,gas;fatty acids,volatile;Red Star Erguotou;volatile components
基金项目(Foundation):
作者(Author):
胡朝阳,裘璐,肖海涛
HU Chaoyang,QIU Lu,XIAO Haitao(School of Pharmacology
DOI: 10.19367/j.cnki.1000-2707.2010.04.016
参考文献(References):
- [1]张宏波,刘鸿雁.大庆老窖白酒直接进样GC/MS定性定量分析[J].酿酒,2005(32):86.
- [2]Mondello L,Tranchida PQ,Dugo P,et al.Comprehensivetwo dimensional gas chromatography-mass spectrometry:areview[J].Mass Spectrom Rev,2008(27):101-124.
- [3]王光辉,熊少翔.有机质谱解析[M].北京:化学工业出版社,2005:51-71.
- [4]庄名扬.中国白酒香味物质形成机理及酿酒工艺的调控[J].酿酒,2007(2):109-113.
- [5]王沙木.气相色谱法测定白酒中乙酸乙酯含量的探讨[J].黑龙江科技信息,2007(2):30.
- [6]李霞,柳玉英.白酒中醛类物质的光度法测定[J].山东理工大学学报(自然科学版),2006(1):71.
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