李零;郝小燕;肖海涛;张旭;
LI Ling,HAO Xiao-yan,XIAO Hai-tao,ZHANG Xu,(School of Pharmacy,Guiyang Medical College,Guiyang 550004,China)

• 1:贵阳医学院药学院
• 2:贵阳医学院药学院
• 3:贵阳医学院药学院
• 4:贵阳医学院药学院 贵州贵阳550004

摘要(Abstract)：

目的:分离鉴定地榆中的指标性成分,并对妇科再造丸中该指标性成分进行薄层鉴别。方法:运用现代分离纯化技术和波谱方法分离、鉴定指标性化合物,用薄层色谱法(TLC)鉴别妇科再造丸中的地榆。结果:指标性化合物经结构鉴定为地榆苷-Ⅰ,其化合物可作为妇科再造丸中地榆薄层鉴别的依据。结论:地榆苷-Ⅰ作为指标性成分鉴别妇科再造丸中的地榆,方法灵敏,重现性好,专属性强。
Objective: To develop a method for isolation and identification of index components from radix of Sanguisorba officinalis L.in Fukezaizao pill.Methods: The index components were purified by column chromatography and elucidated by spectroscopy,The radix of Sanguisorba officinalis L.in Fukezaizao pill was identified by TLC. Results: the index component was elucidated as ziyuglycoside-I,which can be used in the identification of radix of Sanguisorba officinalis L.in Fukezaizao pill by TLC.Conclusions: Using ziyuglycoside-I as index component,radix of Sanguisorba officinalis L.in Fukezaizao pill can be identified by TLC.This method is sensitive,reproducible and highly characteristic.

关键词(KeyWords)： 植物制剂;中草药;色谱法,薄层;地榆;地榆苷-Ⅰ;妇科再造丸
plant preparation;drugs,Chinese herbal;chromatography,thin layer;Sanguisorba officinalis L.;ziyuglycoside-I;Fukezaizao pill

Abstract:

Keywords:

基金项目(Foundation): 贵州省中药现代化专项项目[黔科合中药专字(2003)10号]

作者(Author): 李零;郝小燕;肖海涛;张旭;
LI Ling,HAO Xiao-yan,XIAO Hai-tao,ZHANG Xu,(School of Pharmacy,Guiyang Medical College,Guiyang 550004,China)

Email:

DOI: 10.19367/j.cnki.1000-2707.2006.01.019

参考文献(References)：

• [1]江苏新医学院.中药大辞典[M].上册.上海:上海科学技术出版社,1997:807.
• [2]国家药典委员会.中华人民共和国药典[M].一部.北京:化学工业出版社,2005:83.
• [3]曹爱民.地榆中皂苷类化合物分离、鉴定及其含量测定[J].中草药,2003,34(5):397-399.

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