贵州医科大学学报

2008, No.131(02) 176-178

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爱福宁合剂质量标准的研究
A Study on Quality Standard of Aifuning Oral Liquid

张珏;刘丽娜;李勇军;何迅;
ZHANG Jue,LIU Lina,LI Yongjun,HE Xun(School of Pharmacology,Guiyang Medical College,Guiyang 550004,Guizhou,China)

摘要(Abstract):

目的:建立爱福宁合剂质量标准。方法:采用薄层色谱法鉴别苦参、金荞麦,采用高效液相色谱法测定苦参碱的含量。结果:薄层斑点清晰,重现性好,含量测定平均回收率为99.35%,RSD为1.52%。结论:该方法准确,简便,重现性好,可用于该制剂的质量控制。
Objective:To establish a quality control standard for Ai Funing oral liquid.Methods:Radix Sophorae Flavescentis and Rhizoma Fagopyri Dibotryis were identified with thin-layer Chromatography(TLC) and the content of matrine was determined with high pressure liquid chromatography(HPLC) in the preparation.Results:The TLC developed spots were fairly clear,the HPLC method showed good repeatability,and the average recovery of matrine was 99.35% with RSD 1.52%(n=9).Conclusions:The method is accurate,rapid,sensitive with good reproducibility,which is a an ideal method for quality control of Aifuning oral liquid.

关键词(KeyWords): 苦参碱;爱福宁合剂;色谱法,高压液相;色谱法,薄层
sophocarpidine;aifuning oral liquid;chromatography,high pressure liquid;chromatography,thin layer

Abstract:

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作者(Author): 张珏;刘丽娜;李勇军;何迅;
ZHANG Jue,LIU Lina,LI Yongjun,HE Xun(School of Pharmacology,Guiyang Medical College,Guiyang 550004,Guizhou,China)

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DOI: 10.19367/j.cnki.1000-2707.2008.02.020

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