贵州医科大学学报

2004, (06) 497-498

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莫达芬尼酸及莫达芬尼砜的核磁共振波谱研究
A Study on Nuclear Magnetic Resonance Spectrum of Modafinil Acid and Modafinil Sulfone

陆江海,王杉,崔凯荣,邓静,吴侔天,张长久
LU Jiang hai, WANG Shan, CUI Kai rong, DENG Jing, WU Mou tian, ZHANG Chang jiu (Drug Test Center, State Institute for Sports Medicine, Beijing 100029, China)

摘要(Abstract):

目的 :对莫达芬尼酸和莫达芬尼砜进行核磁共振波谱 (NMR)研究。方法 :采用 1D NMR(1H、13 C NMR、DEPT)和 2D NMR(1H 1HCOSY、HMQC、HMBC)等现代核磁技术检测莫达芬尼酸和莫达尼酸的结构。结果 :归属了莫达芬尼酸和莫达芬尼砜的H、C谱线。结论 :首次报道了莫达芬尼酸和莫达芬尼砜的碳谱数据。
Objective: To study the nuclear magnetic resonance(NMR)spectrum of modafinil acid and modafinil sulfone. Methods: Complete 1H NMR and 13 C NMR assignments of these compounds were carried out using DEPT, HMQC and HMBC techniques. Results: The H and C NMR spectra of the two compounds were sorted. Conclusion: The 13 C NMR data of them are reported for the first time. [

关键词(KeyWords): 莫达芬尼酸;莫达芬尼砜;磁共振波谱学
modafinil acid; modafinil sulfone; magnetic resonance spectrum analysis,mass

Abstract:

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作者(Author): 陆江海,王杉,崔凯荣,邓静,吴侔天,张长久
LU Jiang hai, WANG Shan, CUI Kai rong, DENG Jing, WU Mou tian, ZHANG Chang jiu (Drug Test Center, State Institute for Sports Medicine, Beijing 100029, China)

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DOI: 10.19367/j.cnki.1000-2707.2004.06.010

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